Course

Instrumental Analysis (MLJ540)

The course provides an introduction to instrumental analysis with focus on the entire analytical process from raw sample to calculated result.


Course description for study year 2020-2021. Please note that changes may occur.

See course description and exam/assesment information for this semester (2024-2025)

Semesters

Facts

Course code

MLJ540

Credits (ECTS)

10

Semester tution start

Autumn

Language of instruction

English

Number of semesters

1

Exam semester

Autumn

Content

The course provides an introduction to instrumental analysis with focus on:

            - Organic chemistry, calculations and validation

            - Sample preparation

            - Organic analysis and very briefly inorganic analysis

            - Detectors and detector principles

            - Separation science

The course provides an introduction to instrumental analysis with main focus on organic chemistry, calculations and validation, sample preparation, atomic absorption/emission spectroscopy, UV-VIS-spectroscopy, fluorescence-spectroscopy, IR-spectroscopy, mass spectrometry (MS), gas chromatography (GC) and liquid chromatography (HPLC).

Learning outcome

The students will learn:

- General organic chemistry (solvents, solubility, buffers)

- Quantitative and qualitative analysis (units, calibration, calculations and validation)

- Sample preparation (mechanical and chemical)

- Organic analysis and briefly inorganic analysis

- Detectors and detector principles

- Separation science (separation principles, gas chromatography and liquid chromatography)

Students will be introduced to general sample preparation techniques as well as the principles of instrumental analysis and to construction of modern analytical instruments. Topics within general organic chemistry, calculations, calibration and method validation will give students insight in the analytical process from raw sample to final result. Instrumental methods covered are: Atomic absorption/emission spectroscopy, UV-VIS-spectroscopy, fluorescence-spectroscopy, IR-spectroscopy, mass spectrometry (MS), gas chromatography (GC), liquid chromatography (HPLC) and immunoaffinity methods.

Required prerequisite knowledge

HSE-course for master students (TN501)

General chemistry, and basic statistics.

Undergraduate laboratory courses.

Recommended prerequisites

General chemistry, organic chemistry, analytical chemistry and basic statistics.

Experience in basic laboratory work and some analytical chemistry laboratory work.

Exam

Form of assessment Weight Duration Marks Aid Exam system Withdrawal deadline Exam date
Home exam 3/4 4 Hours Letter grades Inspera assessment 17.11.2020
Laboratory exercises 1/4 Letter grades


Both the practical part and the exam has to be passed to pass the course. Practical work from previous years may be accepted.

Coursework requirements

Completion of mandatory lab assignments are to be made at the times and in the groups that are assigned and published on Canvas. Absence due to illness or for other reasons must be communicated to the laboratory personnel as soon as possible. One cannot expect that provisions for completion of the lab assignments at other times can be made, unless prior arrangements with the laboratory personnel have been agreed.

Failure to complete the assigned labs on time or not having the reports approved will result in barring from taking the final course exam.

Course teacher(s)

Coordinator laboratory exercises:

Liv Margareth Aksland

Course coordinator:

Cato Brede

Coordinator laboratory exercises:

Kjetil Bårdsen

Course teacher:

Mark van der Giezen

Method of work

4 hours lectures per week or 4-8 hours of laboratory work during the three lab-weeks. Project work with written reports.

Overlapping courses

Course Reduction (SP)
Instrumental analysis (MET240_1) , Instrumental Analysis (MLJ540_1) 10
Instrumental Analysis (MLJ540_1) , Instrumental analysis (MOT130_1) 10
Instrumental Analysis (MLJ540_1) , Instrumental analysis (TE6026_1) 6
Instrumental Analysis (MLJ540_1) , Instrumental analysis (TE6026_A) 6

Open for

The course is available for master students in Biological Chemistry, Environmental Engineering and Environmental Monitoring in the Northern Regions.

Other students may be accepted as long as they fulfill the admission requirements, and there is available capacity in the lab part of the course.

Course assessment

Usually by forms and/or discussion according to university regulations

Literature

Skoog, D. A. (2017). Principles of instrumental analysis (F. J. Holler & S. R. Crouch, Red.; 7th edition). Cengage Learning.
The course description is retrieved from FS (Felles studentsystem). Version 1